ISO 21561-1:2015

Published (Edition 1, 2015)

This publication was last reviewed and confirmed in 2020. Therefore this version remains current.

ISO 21561-1:2015

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Abstract

ISO 21561-1:2015 specifies procedures for the quantitative determination of the microstructure of the butadiene and the content of styrene in solution-polymerized SBR (S-SBR) by 1H-NMR spectrometry as an absolute method and by IR spectrometry as a relative method. The styrene content is expressed in mass % relative to the whole polymer. The trans, cis and vinyl contents are expressed in mol % relative to the butadiene. These methods are applicable only for raw rubber.

NOTE 1 IR spectrometry can also give absolute values of microstructure by calibration with S-SBRs of known absolute microstructure obtained by 1H-NMR spectrometry.

NOTE 2 Only "vinyl", "trans" and "cis" are used in this part of ISO 21561. However, the expression of vinyl, trans and cis mean as follows in general:

- vinyl: vinyl unit, vinyl bond, 1,2-unit, 1,2-bond, 1,2-vinyl-unit or 1,2-vinyl-bond;

- trans: 1,4-trans unit, 1,4-trans bond, trans-1,4 unit or trans1,4 bond;

- cis: 1,4-cis unit, 1,4-cis bond, cis-1,4 unit or cis-1,4 bond.

General information

Status
: Published

Publication date
: 2015-07

Stage
: International Standard confirmed [90.93]
Edition
: 1

Number of pages
: 17
Technical Committee :
ISO/TC 45/SC 3

ICS :
83.060
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